Effect of Green Synthesis Clay Nano Composite Material on Reactive Dye of Methyl Orange

Textile is a leading industry of every country because of necessity of clothes and a textile industry plays a vital role in the industrial sectors and it consume lots of water for their usage as well as they dispose equal amount of wastewater with toxic dye contents.

When textile wastewater is disposed to natural system, it creates major impacts to human as well as natural environment such as human related diseases, pollution of natural system etc.,

So, it is necessary to treat them effectively for the purpose of protection of Environmental condition and also to save humans and animal life. The Ocimum Tenuiflorum (Tulsi) leaves extract arbitrated green synthesis of silver coated nanoparticles (AgNPs) was used as an adsorbent for dye removal.

Isolation and Characterisation of Alkaloid from Leaves of Brugmansia Candida

One of alkaloid compound was isolated from leaves Brugmansia candida. The compound was purified by chromatography column with silica gel as adsorbent. The purity of the isolated compound was tested by TLC, melting point.

The structure of the compound was identified by means of spectroscopic include Ultraviolet Spectroscopy, Infrared Spectroscopy, and NMR. All data obtained indicates that the resulting compound is an isoquinolin alkaloid.

The use of plant as a medicine related with chemistry compound had by the plant mainly the bioactive one. Bioactive compound can be found at fruit, flower, leaf, root, and trunk. Bioactive compound in the plant is a secondary metabolic compound such as alkaloid, flavonoid, steroid, and saponin .

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Synthesis and Characterization of Boron and 2-Aminophenol Schiff Base Ligands with Their Cu(II) and Pt(IV) Complexes and Evaluation as Antimicrobial Agents

Synthesis, Characterization and biological study of two Schiff base ligands derived from 2-aminophenol and 4 bromoacetophenone (1:1) (L1) and boron Schiff base which was derived from L1 and sodium borohydride (1:1) (L2).

Cu (II) and Pt (IV) complexes of the Schiff base ligands were synthesized. The prepared compounds have been investigated by molar conductivity, elemental analysis, FTIR, 1H 13 CNMR, thermal analysis, UV-VIS, as well as atomic absorption and magnetic susceptibility.

The biological study of the ligands and their metal complexes were carried out against E-coli, Staphylococcus, as bacteria species, Candida and Mycrosporium Canis as fungi.  

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Experimental and Theoretical Investigation of the Molecular and Electronic Structure of 3-Acetoxy-2-Methylbenzoic Acid using Quantum Chemical Computational Calculations

In this work, experimental and theoretical study on the molecular structure of 3-acetoxy-2-methyl benzoic acid (3A2MBA) is performed based on the quantum mechanical approach by density functional theory (DFT) calculations.

The optimized geometrical parameters were done by DFT using the B3LYP method show good agreement with experimental X-ray data. The vibrational harmonic frequencies were scaled using scale factors, yielding a good agreement between the experimentally recorded and the theoretically calculated values with the aid of a calculation of the Total energy distribution (TED).

The population of electrons in core, valance and Rydberg sub-shells has been predicted. The natural hybrid atomic orbital studies enhance us to know about the type of orbitals and its percentage of s-type and p-type character.

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The Mathematical Description of the Electro Polymerization of the ComplexForming Monomers over Transition Metals

The choosing of the monomer for the resulting conducting polymer is determined by how the polymer materials are going to be used.

For example, the polymers, used as corrosion protecting coatings, have to be stable and adherent, and those used in sensors and biosensors must possess affinity to the analyte.

On the other hand, other monomers may have their electropolymerization on some metals accompanied by the complex formation. This phenomenon has already been observed during the electrochemical modification of the organic compounds and during their electropolymerization.

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Prediction of Melting Point and Aqueous Solubility of Barbiturates

Classical Barbiturates are formed by substituting one or both hydrogen atoms at the 5-position with alkyl, aryl, and/or alicyclic groups.

In this study, a previously develop ed UPPER (Unified Physicochemical Property Estimation Relationships) approach is applied to predict the melting points and aqueous solubilities of a series of barbiturates.

The descriptors from a previously developed UPPER model on hydrocarbons are used to generate new descriptors for barbiturate ring using multiple linear regression analysis. Melting points can be predicted solely from additive enthalpic and non-additive entropic descriptors.

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An Evaluation of Anti-Microbial Pattern of Escherichia coli Isolated from Clinical Samples at a Tertiary Care Hospital

Antibiogram is the periodic evaluation of antimicrobial susceptibility pattern of bacterial isolates in a local area. It helps clinicians in selecting antimicrobials for empirical therapy and monitors the development of resistance.

This study is a move to determine the antimicrobial susceptibility pattern of E. coli from urine, exudate and blood samples. It is a retrospective review of in-patient culture results of urine, exudate and blood samples were investigated from January 2015 to December 2015.

A total of 254 reports were obtained for analysis of antimicrobial susceptibility for 19 antibiotics. Out of the total 254 E. coli isolates, the highest number of positive E. coli isolates were found among urine samples (74%) followed by exudates (21%) and blood (5%).

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Chemopreventive Efficacy of Fisetin against Benzo(a)pyrene Induced Lung Carcinogenesis in Experimental Animals Swiss Albino Mice

The present study was designed to evaluate the effects of oral administration of the fisetin on lung tumour initiation by orally applied Benzo(a)pyrene (B(a) P).

Its effects on biochemical markers enzymes as well as pathological markers were evaluated. The pathological enzyme activities were increased (P<0.05) in lung cancer bearing animals when compared with control group animals.

Fisetin-treated animals from groups-3 and- 4 showed a significant (P<0.05) decreases in the levels of these enzymes when compared to B(a)P induced group-2 animals. Levels of glycoprotein and activities of membrane ATPases play an important role in the carcinogenesis.

Green Synthesis of Copolymer Electrolytes for Lithium Batteries Catalyzed by an Ecocatalyst Maghnite-H+

The ideal electrolyte material for a solid-state battery would have the ionic conductivity of a liquid, the mechanical properties of a solid, and the formability of a commodity thermoplastic.

The ionic conductivity changed with the molecular weight of the polymer, it varies inversely with the glass transition temperature. In our study, to achieve high ionic conductivity, we synthesize copolymer PDMS/PEO as polymer electrolytes by a simple method.

One step of catalytic ring opening polymerization using Maghnite-H+ (Mag-H+), a montmorillonite sheet silicate clay exchanged with protons. It is preferred for its many advantages: a very low purchase price compared to other catalysts, the easy removal of the reaction mixture.

Determination of Mineral Composition of Some Wild Edible Plants Consumed by Bodos of Assam, North-East India

In the present study, the macro and micro elements present in eleven wild edible plants consumed by Bodos of Assam from North-East India were assessed.

The study showed variable amounts of minerals content among the plant species which are presented herein and discussed. The heavy metals like cadmium and arsenic were not detected in the plant species.

The investigation showed that these non-conventional food sources are good sources of minerals and consumption of such vegetables can replace the malnutrition problems.

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Study of Intermolecular Interaction in Risperidone and Polyethylene Glycol Suspension

The speed of sound can be considered to evaluate acoustical parameters and hence, to investigate physico-chemical properties of drug polymer suspension.

Investigations of these physico-chemical properties enable to understand the nature and strength of particle-liquid interactions. The suspensions were made up of a 1:1, 1:2, 1:3, 1:4, 1:5 mixtures by weight of drug Risperidone and Polyethylene Glycol by using ultrasonic probe sonicator.

The product was further characterized by using techniques such as scanning electron microscopy (SEM), fourier transform infrared spectrocopy (FTIR). Ultrasonic velocity, density, and viscosity have been measured for different

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RP-UPLC Method for the Simultaneous Quantification of Related Substances in Emtricitabine, Tenofovir Disoproxil Fumarate and Efavirenz Pharmaceutical Dosage Forms

A stability-indicating reverse phase ultra-performance liquid chromatography (RP-UPLC) method, developed for the simultaneous quantification of eight related compounds in the dosage forms of Emtricitabine, Tenofovir Disoproxil Fumarate and Efavirenz.

Efficient chromatographic separation was achieved on an Acquity UPLC BEH Phenyl (2.1×100 mm, 1.7 m) column using mobile phase A (Buffer, 1.0 mL of TEA in 1000 mL of water pH adjusted to 4.0 ± 0.05 with diluted OPA) and mobile phase B in gradient mode with the flow rate of 0.5 mL/min and the peaks were monitored at 265 nm.

In the developed method, the resolution of Emtricitabine, Tenofovir Disoproxil Fumarate, Efavirenz and related substances were found to be greater than 2.0.

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Molecular Docking Studies of Quinones against Human Inducible Nitric Oxide Synthase

Quinones represent an important class of naturally occurring compounds that are present in flowering plants, bacteria and fungi, primarily as essential components of the electron-transport chains involved in photosynthesis and cellular respiration.

There are various kinds of biological activities such as antineoplastic, antimalarial, antitumor, anticoagulant, herbicidal and antibiotic attributable to this group of compounds including their derivatives.

Synthetic or natural quinoid compounds such as 1, 4-benzoquinone and 1, 4-naphthoquinone have been used as dyes. Some quinones are widely applied in the fields of photochemistry, co-ordination chemistry and synthetic chemistry.

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Review on Benefits of Drug Information Center Services

Hospital is a multiple health care institution provides patient care with the support of specialized medical and Para medical team. The drug information center (DIC) plays a key role in hospitals solving several drug problems and releases the news letters relates to information about the drugs, diseases, patient safety and cost effectiveness of drug DIC guides, safeguards the health care professionals to the right practice of the patient’s community.

It offers a learning based center for health care professionals to acquire skills and knowledge necessary for conducting research and delivery of exact evidence based drug information to the community.

The drug information center routinely receives queries from hospital staff, patients and responds to queries regarding adverse drug reactions, drug interactions, pharmacokinetic parameters of drugs, information on new drugs available in the market.

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Novel Acrylic Copolymers Derived from 4-Chloro-3,5-Dimethyl Phenol

A      series of methacrylate polymers derived from 4-chloro-3,5-dimethyl phenyl methacrylate (CDMPMA) with comonomer tetrahydrofurfuryl methacrylate (THFMA) were synthesized via free radial polymerization technique.

The copolymers were characterized by fourier transform infrared spectroscopy (FTIR), nuclear magnetic resonance spectroscopy (1H-NMR), thermogravimetric analysis (TGA) and gel permeation chromatography (GPC). All polymers were thermally stability up to 200ºC under nitrogen atmosphere.

The reactivity ratio of monomers in copolymer was obtained by different linearization methods using 1H NMR data. Antimicrobial activities of the homopolymers and copolymers were investigated for various microorganisms such as bacteria, fungi and yeast.

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A Novel Stability Indicating RP-HPLC Method for Simultaneous Estimation of Atazanavir and Cobicistat in Bulk and Pharmaceutical Dosage Forms

Reverse phase high performance liquid chromatographic method has been focused with the aim of reducing analysis time and maintaining good efficiency.

The present work describes a rapid, simple, precise, selective stability indicating RP-HPLC method for simultaneous estimation of Atazanavir and Cobicistat in tablet dosage forms.

A Phenomenix C8 column of 250 × 4.6 mm internal diameter, 5 µm particle size with mobile phase consisting of O.1 M ammonium acetate and methanol of HPLC grade in the ratio of 1:1 was used. The flow rate was maintained at 1.2 ml/min. The effluents were monitored at 268 nm.

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The Structure Elucidation of a Component in Essential Oil of Citrus Reticulata Blanco Peel by its Mass Spectrum

A peak including an unknown component in the total ion chromatogram of essential oil from Citrus reticulata Blanco peel, which retention index is nearly the same as that of tetradecanoic acid (1748) in apolar column, can’t match a suitable compound through the searching of NIST08 (National institute of science and technology) MS (mass spectrum) database.

Its’ structure was tentatively elucidated by the mass spectrum. In the end, the most probably identity was deduced, and its correction will be confirmed in the following research.

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